SUPER CAPACITORS REPRESENT A NEW CLASS OF ENERGY STORAGE DEVICES THAT HAVE BEEN ATTRACTED MANY RESEARCHERS IN LAST FEW YEARS. GRAPHENE WITH UNIQUE PROPERTIES SUCH AS SUPERIOR ELECTRICAL CONDUCTIVITY AND LARGE SPECIFIC SURFACE AREA IS ONE OF THE MOST SUITABLE MATERIALS IN SUPER CAPACITOR APPLICATIONS [1]. BESIDES, METAL OXIDES ARE BEING USED AS ACTIVE COMPOUNDS IN SUPER CAPACITORS DUE TO THEIR ROLE IN REDOX REACTIONS. IN THIS RESEARCH, SYNTHESIS AND CHARACTERIZATION OF SUPER CAPACITOR ELECTRODES BASED ON GRAPHENE AND MNO2 NANOSTRUCTURED MATERIALS WAS STUDIED UNDER DIFFERENT CONDITIONS. FOR THIS PURPOSE, GRAPHENE OXIDE (GO) WAS SYNTHESIZED BY HUMMERS’ METHOD AND THEN, IT WAS DEPOSITED ON A NICKEL FOAM VIA ELECTROPHORETIC PROCESS WITH APPLIED POTENTIAL OF 5 V IN SOLUTION CONTAINING MGSO4 AND GO [2]. FINALLY, MNO2 ANODICALLY ELECTRODEPOSITED ON REDUCED GO/NI-FOAM BY USING SUCCESSIVE CYCLIC VOLTAMMETRY (CV) AT THE SCAN RATE OF 0.1 VS-1 IN 5 CYCLES. MORPHOLOGY AND CHEMICAL COMPOSITION OF THE PREPARED ELECTRODE WERE INVESTIGATED BY SCANNING ELECTRON MICROSCOPY (SEM) AND X-RAY PHOTOELECTRON SPECTROSCOPY (XPS), RESPECTIVELY. THE ELECTROCHEMICAL AND CAPACITIVE PROPERTIES OF THE SYNTHESIZED SUPER CAPACITOR ELECTRODES WERE STUDIED IN A THREE- ELECTRODES SYSTEM USING VARIOUS TECHNIQUES INCLUDING CV IN THE POTENTIAL WINDOW OF 0 TO 1.0 V (FIG. 1), CHARGE- DISCHARGE (CD) AT A CONSTANT CURRENT OF 6 MA (FIG. 2), AND THE ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY (EIS), ALL IN 1.0 M NA2SO4 SOLUTION. THE RESULTS SHOWED THAT THE SYNTHESIZED MNO2/RGO SUPER CAPACITOR ELECTRODE EXHIBITED A CAPACITANCE OF 273 FG-1.